62-13-5
- Product Name：Adrenalone hydrochloride
- Molecular Formula：C9H11NO3.HCl
- Purity：99%
- Molecular Weight：217.652
Product Details
Melting Point:244-249 °C (dec.)
Purity:99%
Reliable factory customized supply Adrenalone hydrochloride 62-13-5
- Molecular Formula:C9H11NO3.HCl
- Molecular Weight:217.652
- Vapor Pressure:3.7E-07mmHg at 25°C
- Melting Point:244-249 °C (dec.)
- Boiling Point:405.6 °C at 760 mmHg
- Flash Point:199.1 °C
- PSA：69.56000
- LogP:1.69280
Adrenalone hydrochloride(Cas 62-13-5) Usage
|
Preparation |
Obtained by action of hydrochloric acid on 3,4-dihydroxy-a-methylaminoacetophenone (65%), in methanol. |
InChI:InChI=1/C9H11NO3.ClH/c1-10-5-9(13)6-2-3-7(11)8(12)4-6;/h2-4,10-12H,5H2,1H3;1H
62-13-5 Relevant articles
Production process of adrenal glands
-
Paragraph 0031-0032, (2021/11/15)
The invention discloses a production tec...
Preparation method of adrenalone hydrochloride
-
Paragraph 0014; 0034; 0035; 0039; 0040; 0044; 0045, (2017/07/21)
The invention relates to a preparation m...
PROCESS FOR THE PREPARATION OF OPTICALLY ENRICHED ADRENALINE
-
Paragraph 0046-0056, (2016/06/01)
A process for the production of (-)-adre...
62-13-5 Process route
-
-
99-40-1
2-chloro-3',4'-dihydroxyacetophenone
-
-
74-89-5
methylamine
-
-
62-13-5
1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamino-ethan-hydrochlorid
| Conditions | Yield |
|---|---|
|
2-chloro-3',4'-dihydroxyacetophenone; methylamine;
In
water; acetonitrile;
at 0 - 40 ℃;
for 3h;
Large scale;
With
hydrogenchloride;
In
methanol; isopropyl alcohol;
at 5 - 25 ℃;
for 1.5h;
Large scale;
|
56% |
|
2-chloro-3',4'-dihydroxyacetophenone; methylamine;
In
ethanol;
at 10 - 45 ℃;
Large scale;
With
hydrogenchloride;
In
ethanol; water;
at 0 - 10 ℃;
for 5h;
Large scale;
|
50 kg |
-
-
99-45-6
adrenalone
-
-
62-13-5
1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamino-ethan-hydrochlorid
| Conditions | Yield |
|---|---|
|
With
hydrogenchloride;
In
ethanol;
for 0.5h;
pH=2-3;
|
86.9% |
62-13-5 Upstream products
-
99-40-1
2-chloro-3',4'-dihydroxyacetophenone
-
74-89-5
methylamine
-
99-45-6
adrenalone
-
120-80-9
benzene-1,2-diol
62-13-5 Downstream products
-
104819-56-9
R,S-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamido-ethan
-
132225-51-5
α-(p-cyano-N-methylbenzamido)-3,4-dihydroxyacetophenone
-
104819-56-9
R-(+)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamido-ethan
-
104819-56-9
S-(-)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-methylamido-ethan
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